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Monday, 21 December 2015

Effect of re-extraction parameters and drying temperature on the antioxidant properties and dietary fiber of Red sorrel (Hibiscus sabdariffa L.) calyces residues

Volume 74, 15 November 2015, Pages 680–688

Highlights

Residues of Hibiscus sabdariffa L. are rich in dietary fiber (DF) and antioxidants.
Effect of re-extraction on DF and antioxidants of the residue was analyzed using RSM.
Even after 3 re-extraction steps, the residues are richer in DF and antioxidants.
Residues possessed better antioxidant fibers than fruit pomace and peel fiber.
These residues can be potential source of DF and antioxidants for food industry.

Abstract

Effect of re-extraction and drying temperature on the antioxidant capacity and dietary fibers of Hibiscus sabdariffa L. calyces residues were studied using response surface methodology with respect to 3 factors Doehlert experimental design. Mathematical models were obtained for the effect of re-extraction parameters on ascorbic acid, TPC, TFC, ABTS, SDF, and SDF/IDF ratio. The suitability of each response model was judged using the average absolute deviation method and the calculation of the Bias factors. No significant difference was observed for the total dietary fiber content among different samples. Soluble dietary fibers in the residues varied from 47 to 216 g kg−1 dry matter. Insoluble dietary fiber represented more than 75% of total dietary fibers. Samples exhibited high scavenging activity of ABTS cation radical (TEAC ranging from 2.488 to 9.416 mMeq. Trolox) and DPPH free radical with IC50 values ranging from 0.915 to 0.062 mg mL−1. TEAC and IC50 values were correlated to TPC and TFC. The study indicated that H. sabdariffa L. calyces residues can be a potential source of additive/ingredient for the food industry and the re-extraction at lower temperatures further improves the dietary fiber composition of the residue.

Graphical abstract

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Keywords

  • Hibiscus sabdariffa L.;
  • Re-extraction;
  • Ascorbic acid;
  • Antioxidant activity;
  • Dietary fibers;
  • RSM

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