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Saturday, 12 December 2015

Preparation and characterization of flax biocomposites made of seed mucilage reinforced by fibers

  • a University of Rouen, UMR 6270 CNRS, FR 3038, 76821 Mont-Saint-Aignan Cedex, France
  • b Department of Oil and Fiber Crops, NI Vavilov Research Institute of Plant Industry, Saint-Petersburg, Russia
  • c LBN Flax Scutching Company, Le Bocasse, France
  • d University of Le Havre, LOMC UMR 6294 CNRS, 76058 Le Havre Cedex, France
  • e University of Brighton, School of Pharmacy, BN2 4AT Brighton, United Kingdom

Abstract

Natural biocomposites were prepared from flax fibers and mucilage polysaccharides extracted from flax seeds, as a matrix, in two steps: impregnation and compression molding. The ribbons were preimpregnated with water plasticized mucilage. Solid mucilage (30%, w/w) was added to the ribbon impregnated with 20% mucilage, and the composite was compression molded. The solidified mucilage was homogeneous and rigid (2 GPa) with an elastic deformation of approximately 1%. The mechanical properties of the composites were in the ranges of 7–10 GPa, 300–400 MPa and 4–5% for the modulus, maximal strength and strain, respectively. The two latter parameters were larger than the ones for the fiber. The experimental values of the modulus and strength were in accordance with the values computed using the rule of mixture, which indicated a good interface between the fibers and the matrix. This was confirmed visually with scanning electron microscopy. The water sorption behavior of the composites was intermediate between the mucilage and the fiber alone.

Keywords

  • Fabrics/textiles;
  • Mechanical properties;
  • Mechanical testing;
  • Compression moulding

Corresponding author. Tel.: +33 2 35 14 66 94; fax: +33 2 35 14 67 04.